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Scandinavian Journal of Clinical and Laboratory Investigation

ISSN 0036-5513

2 papers in the library · 107 citations · publishing 2008-2013

Papers

Identification of novel psychoactive drug use in Sweden based on laboratory analysis – initial experiences from the STRIDA project

Scandinavian Journal of Clinical and Laboratory Investigation May 22, 2013 Anders Helander, Olof Beck, Robert Hägerkvist et al. 82 citations

New psychoactive substances, sold online as 'legal highs' or disguised as 'bath salts' and 'plant food', are increasingly used by young people in Sweden. In a project monitoring these drugs, urine and blood samples from 103 emergency department cases of suspected recreational drug intoxication were analyzed. Psychoactive substances were detected in 82% of cases; 78% of subjects were 25 or younger, and 81% were male. Detected substances included synthetic cannabinoids, substituted cathinones, tryptamines, plant-based substances, and conventional drugs. In 44% of cases, more than one new or conventional drug was present. The findings document widespread use of diverse new psychoactive substances among Swedish youth.

Determination of amphetamine, methamphetamine, MDA and MDMA in human hair by GC‐EI‐MS after derivatization with perfluorooctanoyl chloride

Scandinavian Journal of Clinical and Laboratory Investigation October 21, 2008 Sys Stybe Johansen, Jakob Jornil 25 citations

A quantitative gas chromatography–mass spectrometry method was developed to measure amphetamine, methamphetamine, MDA, and MDMA (ecstasy) in human hair. The procedure uses liquid-liquid extraction of hydrolyzed hair with deuterated internal standards and derivatization with perfluorooctanoyl chloride. Validation showed a linear range of 0.25 to 25 ng/mg, intra-day precision of 3–6% RSD, inter-day precision of 3–17% RSD, and trueness between 96% and 106%. Detection limits ranged from 0.07 to 0.14 ng/mg and quantification limits from 0.24 to 0.46 ng/mg. Applied to 40 authentic hair samples, concentrations ranged up to 3.2 ng/mg for amphetamine, 0.4 ng/mg for MDA, and 5.9 ng/mg for MDMA; methamphetamine was detected once at trace level. The method is simple, robust, and sensitive enough for measuring these drugs in abusers' hair.