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Determination of Lysergic Acid Diethylamide (LSD) in Urine by Instrumental High-Performance Thin-Layer Chromatography

Lee M. Blum, E F Carenzo, Fredric Rieders

Journal of Analytical Toxicology September 1, 1990 DOI: 10.1093/jat/14.5.285 via OpenAlex

Summary

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A high-performance thin-layer chromatography method can detect less than one microgram of LSD per liter of urine after a single-step extraction with an alkaline wash. The technique is compared with radioimmunoassay for measuring LSD in urine.

Study at a glance

Characteristics Method development and comparison Peer reviewed
Topics LSD
Keywords Urine Extraction chemistry Radioimmunoassay Thin-layer chromatography
Citations 15
Key finding The HPTLC technique can detect less than 1 microgram of LSD per liter of urine.

Abstract

An instrumental high-performance thin-layer chromatographic (HPTLC) technique for the determination of lysergic acid diethylamide (LSD) in urine was developed. Before chromatographic separation, a single-step extraction with alkaline wash is performed. The procedure can detect less than 1 microgram LSD/L urine. Results of HPTLC determination are compared with those from a radioimmunoassay (RIA) procedure.

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